样品前处理技术在气相色谱分析中的应用进展

doi:10.3724/SP.J.1123.2013.05035

色谱 ›› 2013, Vol. 31 ›› Issue (7): 634-639.DOI: 10.3724/SP.J.1123.2013.05035

• 特别策划:庆祝欧庆瑜先生八十华诞专栏 • 上一篇下一篇

样品前处理技术在气相色谱分析中的应用进展

严矿林¹, 林丽琼¹, 郑夏汐¹, 肖小华¹, 曹玉娟²

1. 中山大学化学与化学工程学院, 广东广州 510275;
2. 华南师范大学化学与环境学院, 广东广州 510006

收稿日期:2013-05-22 出版日期:2013-07-28 发布日期:2013-07-17
通讯作者: 肖小华, 曹玉娟
基金资助:
广东省自然科学基金项目(S2012010010787).

Progress of sample preparation techniques in gas chromatographic analysis

YAN Kuanglin¹, LIN Liqiong¹, ZHENG Xiaxi¹, XIAO Xiaohua¹, CAO Yujuan²

1. School of Chemistry and Chemical Engineering, Sun Yan-sen University, Guangzhou 510275, China;
2. School of Chemistry and Environment, South China Normal University, Guangzhou 510006, China

Received:2013-05-22 Online:2013-07-28 Published:2013-07-17

摘要/Abstract

摘要：

气相色谱法是当前应用最广泛的分析技术之一。使用气相色谱对复杂基体进行分析时的样品前处理步骤往往繁琐耗时,易引起误差,已成为制约分析效率和准确度提升的关键环节。本文综述了2009-2013年几种主要的样品前处理技术,包括吹扫捕集、固相萃取、固相微萃取、液相微萃取技术以及微波辅助萃取、超声波辅助萃取等场辅助萃取技术在气相色谱分析中的应用研究进展。

关键词: 气相色谱法, 样品前处理, 综述

Abstract:

Gas chromatography (GC) is a widely used analytical technique in many fields. Sample preparation is very important in GC analysis due to its time consumed and deviations produced. In the present paper, the progress of some typical sample preparation techniques in gas chromatography, including purge and trap, solid phase extraction, solid phase microextraction, liquid phase microextraction, microwave assisted extraction, ultrasonic-assisted extraction, etc., are reviewed.

Key words: gas chromatography (GC), review, sample preparation

中图分类号:

O658

严矿林, 林丽琼, 郑夏汐, 肖小华, 曹玉娟. 样品前处理技术在气相色谱分析中的应用进展[J]. 色谱, 2013, 31(7): 634-639.

YAN Kuanglin, LIN Liqiong, ZHENG Xiaxi, XIAO Xiaohua, CAO Yujuan. Progress of sample preparation techniques in gas chromatographic analysis[J]. Chinese Journal of Chromatography, 2013, 31(7): 634-639.

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样品前处理技术在气相色谱分析中的应用进展

Progress of sample preparation techniques in gas chromatographic analysis

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