Progress in sample preparation and analytical methods for trace polar small molecules in complex samples

doi:10.3724/SP.J.1123.2015.08012

Abstract

Abstract:

Small polar molecules such as nucleosides, amines, amino acids are important analytes in biological, food, environmental, and other fields. It is necessary to develop efficient sample preparation and sensitive analytical methods for rapid analysis of these polar small molecules in complex matrices. Some typical materials in sample preparation, including silica, polymer, carbon, boric acid and so on, are introduced in this paper. Meanwhile, the applications and developments of analytical methods of polar small molecules, such as reversed-phase liquid chromatography, hydrophilic interaction chromatography, etc., are also reviewed.

Key words: analytical method, complex samples, polar small molecule, review, sample preparation

CLC Number:

O658

ZHANG Qianchun, LUO Xialin, LI Gongke, XIAO Xiaohua. Progress in sample preparation and analytical methods for trace polar small molecules in complex samples[J]. Chinese Journal of Chromatography, 2015, 33(9): 904-909.

References

[1] Ibrahim M E A, Wahab M F, Lucy C A. Anal Chim Acta, 2014, 820: 187

[2] Montero L, Herrero M, Ibáñez E, et al. J Chromatogr A, 2013, 1313: 275

[3] Self R L, Wu W H, Marks H S. J Agric Food Chem, 2011, 59: 5906

[4] Cui X M, Chen S B, Chen J, et al. Chinese Journal of Analytical Chemistry (崔晓美, 陈树兵, 陈杰, 等. 分析化学), 2013, 41(12): 1869

[5] Magiera S, Baranowski J. J Pharm Biomed Anal, 2015, 109: 171

[6] Wang L, Xu R J, Hu B, et al. Food Chem, 2010, 123: 1259

[7] Li R P, Zhang Y, Lee C C, et al. J Chromatogr A, 2010, 1217: 1799

[8] Tang T, Qian K, Shi T Y, et al. Food Control, 2011, 22: 1203

[9] Sagratini G, Fernández-Franzón M, De Berardinis F, et al. Food Chem, 2012, 132: 537

[10] Johnson J R, Karlsson D, Dalene M, et al. Anal Chim Acta, 2010, 67(8): 117

[11] Wu Y B, Wu J H, Feng Y Q, et al. J Chromatogr B, 2009, 877: 1847

[12] Jégourel D, Delépée R, Breton F, et al. Bioorgan Med Chem, 2008, 16: 8932

[13] Zhu X L, Yang J, Su Q D, et al. J Chromatogr A, 2005, 1092: 161

[14] Bouri M, Lerma-García M J, Salghi R, et al. Talanta, 2012, 99: 897

[15] Sui K, Li J, Wei F, et al. Chinese Journal of Chromatography (隋凯, 李军, 卫锋, 等. 色谱), 2006, 24(2): 152

[16] Zhang M, Tang F L, Fan X K, et al. Chinese Journal of Analytical Chemistry (张明, 唐访良, 范晓开, 等. 分析化学), 2012, 40(10): 1555

[17] Chen L, Chen H. Chinese Journal of Chromatography (陈玲, 陈皓. 色谱), 2003, 21(5): 534

[18] Cai Y Q, Jiang G B, Liu J F, et al. Anal Chem, 2003, 75: 2517

[19] Liu Q, Shi J B, Jiang G B, et al. J Chromatogr A, 2011, 1218: 197

[20] Zhang Q C, Li G K, Xiao X H. Talanta, 2015, 131: 127

[21] Zou J, Song X H, Ji J J, et al. J Sep Sci, 2011, 34: 2765

[22] Liu Y C, Ren L B, Liu Z. Chem Commun, 2011, 47: 5067

[23] Li H Y, Liu Z. TrAC-Trends Anal Chem, 2012, 37: 148

[24] Shao L Z, Yao Y X, Xie M L, et al. Journal of Instrumental Analysis (邵琳智, 姚仰勋, 谢敏玲, 等. 分析测试学报), 2013, 32(12): 1448

[25] Yang X T, Hu Y F, Li G K. J Chromatogr A, 2014, 1342: 37

[26] Jiang L W, Chen Y B, Luo Y M, et al. J Sep Sci, 2015, 38: 460

[27] Duan Y H, Wei Y M. Chinese Journal of Analytical Chemistry (段语晖, 卫引茂. 分析化学), 2013, 41(3): 406

[28] Kosińska A, Andlauer W. Food Chem, 2012, 135: 999

[29] Geng Z M, Yang D, Zhou M P, et al. Food Anal Methods, 2014, 7: 1139

[30] Rodríguez-Gonzalo E, García-Gómez D, Carabias-Martínez R. J Chromatogr A, 2011, 1218: 9055

[31] Hwang B, Wang J, Choong Y. Food Chem, 2003, 82: 329

[32] Redruello B, Ladero V, Cuesta I, et al. Food Chem, 2013, 139: 1029

[33] Li Y, Yang H X, Jin S H, et al. J Chromatogr B, 2013, 929: 33

[34] Önal A, Tekkeli S E K, Önal C. Food Chem, 2013, 138: 509

[35] Loizzo M R, Menichini F, Picci N, et al. Trends Food Sci Technol, 2013, 30: 38

[36] Fernandes J O, Ferreira M A. J Chromatogr A, 2000, 886: 183

[37] Fernandes J O, Judas I C, Oliveira M B, et al. Chromatographia, 2001, 53: S327

[38] Casal S, Mendes E, Fernandes J O, et al. J Chromatogr A, 2004, 1040: 105

[39] Padilla-Sánchez J A, Plaza-Bolaños P, Romero-González R, et al. J Chromatogr A, 2010, 1217: 5724

[40] Marengo E, Gennaro M C, Gianotti V, et al. J Chromatogr A, 1999, 863: 1

[41] Aral H, Aral T, elik K S, et al. Chromatographia, 2014, 77: 771

[42] Ma Y, Kosińska-Cagnazzo A, Kerr W L, et al. J Chromatogr A, 2014, 1356: 64

[43] Tao W W, Duan J A, Yang N Y, et al. Phytochem Anal, 2012, 23: 373

[44] Alpert A J. J Chromatogr A, 1990, 499: 177

[45] Kahsay G, Song H, Van Schepdael A, et al. J Pharm Biomed Anal, 2014, 87: 142

[46] Fu Q, Wang J, Liang T, et al. Chinese Journal of Chromatography (傅青, 王军, 梁图, 等. 色谱), 2013, 31(11): 1051

[47] Karatapanis A E, Fiamegos Y C, Stalikas C D. J Chromatogr A, 2011, 1218: 2871

[48] Jandera P. Anal Chim Acta, 2011, 692: 1

[49] Liang X M. Chinese Journal of Chromatography (梁鑫淼. 色谱), 2011, 29(3): 191

[50] Shen J A, Guo Z M, Liang X M. Progress in Chemistry (沈爱金, 郭志谋, 梁鑫淼. 化学进展), 2014, 26(1): 10

[51] Xu L, Peng R, Guan X M, et al. Anal Bioanal Chem, 2013, 405: 8311

[52] Guo Z M, Lei A W, Liang X M, et al. Chem Commun, 2006: 4512

[53] Qiu H X, Wanigasekara E, Zhang Y, et al. J Chromatogr A, 2011, 1218: 8075

[54] Li Y Z, Nie Z, Wu S M, et al. Journal of Analytical Science (李玉珍, 聂舟, 吴韶敏, 等. 分析科学学报), 2014, 30(4): 537

[55] Fontanals N, Marcé R M, Borrull F. J Chromatogr A, 2011, 1218: 5975

[56] Zhou G S, Pang H Q, Tang Y P, et al. Food Chem, 2014, 150: 260

[57] Pan Y L, Xue P, Li X, et al. Anal Methods, 2013, 5: 6395

[58] Kalili K M, de Villiers A. J Chromatogr A, 2009, 1216: 6274

[59] Bai W Q, Huang H Y, Guo R, et al. Journal of Instrumental Analysis (白万乔, 黄华宇, 郭睿, 等. 分析测试学报), 2014, 33(3): 264

[60] Fang H, Vickrey T L, Venton B J. Anal Chem, 2011, 83