Preparation and performance evaluation of chromatographic column precoated with graphitized carbon black

doi:10.3724/SP.J.1123.2016.10051

Chinese Journal of Chromatography ›› 2017, Vol. 35 ›› Issue (4): 375-381.DOI: 10.3724/SP.J.1123.2016.10051

Previous Articles Next Articles

Preparation and performance evaluation of chromatographic column precoated with graphitized carbon black

WANG Zhonglai¹, SHI Enlin¹, FU Xiaohai¹, ZENG Junling¹, YU Farong²

1. Institute of Public Security Technology, Gansu Institute of Political Science and Law, Lanzhou 730070, China;
2. Key Laboratory of Evidence of Science and Technology Research and Application of Gansu Province, Gansu Institute of Political Science and Law, Lanzhou 730070, China

Received:2016-10-30 Online:2017-04-08 Published:2013-07-30
Supported by:
Natural Science Foundation of Gansu Province (No. 1606RJZA165); Lanzhou Science and Technology Plan Project (No. 2015-3-96); Key Scientific Research Project of Gansu Institute of Political Science and Law(No. GZFXZDLW005).

Abstract

Abstract:

A preparation method of special chromatographic column (LZP-930) for liquor analysis was optimized by precoating the graphitized carbon black (GCB) on the inner wall of fused capillary column. Characteristics of the prepared chromatographic column (LZP-930G) were investigated in detail. The retention behavior was evaluated, and the effect of the precoated GCB on the performance of the LZP-930G column was discussed. Results revealed that the plate number, stability and polarity were increased obviously by using the LZP-930G column, so the separation selectivity and chromatographic peak shape of acids and alcohols were improved. All the 53 compounds in the mixed liquor standard sample could be separated simultaneously. The relative standard deviations of retention times and peak areas were less than 0.63% and 4.51% (n=5), respectively. The result showed that the GCB precoated technology can be used for the preparation of high performance chromatographic column for liquor analysis.

Key words: gas chromatography (GC), graphitized carbon black (GCB), liquor analysis, precoated technology

CLC Number:

O658

WANG Zhonglai, SHI Enlin, FU Xiaohai, ZENG Junling, YU Farong. Preparation and performance evaluation of chromatographic column precoated with graphitized carbon black[J]. Chinese Journal of Chromatography, 2017, 35(4): 375-381.

References

[1] Zhu K Y, Hu J H, Fang Y. Food Research and Development, 2015, 36(21):146朱克永, 胡继红, 方燕. 食品研究与开发, 2015, 36(21):146
[2] Yang J, Lei L B, Hu G Y, et al. Liquor-Making Science and Technology, 2015, 254(8):33杨婧, 雷良波, 胡光源, 等. 酿酒科技, 2015, 254(8):33
[3] Sun Q R, Xiang P, Shen B H, et al. Chinese Journal of Chromatography, 2010, 28(9):833孙其然, 向平, 沈保华, 等. 色谱, 2010, 28(9):833
[4] Yang Y Y, Xie Y F, Tian F F, et al. Chinese Journal of Chromatography, 2013, 31(7):674杨悠悠, 谢云峰, 田菲菲, 等. 色谱, 2013, 31(7):674
[5] Li F F, Yuan L, Wu W Y. Liquor Making, 2015, 42(1):104李芳芳, 袁丽, 吴卫宇. 酿酒, 2015, 42(1):104
[6] Wu J H, Li A J, Huang M Q, et al. Journal of Chinese Institute of Food Science and Technology, 2015, 15(3):194吴继红, 李安军, 黄明泉, 等. 中国食品学报, 2015, 15(3):194
[7] Zhang W W, Liu J X, Han S H, et al. Food Science, 2015, 36(24):122张卫卫, 刘建学, 韩四海, 等. 食品科学, 2015, 36(24):122
[8] Fitzgerald G, James K J, MacNamara K, et al. J Chromatogr A, 2000, 896(1/2):351
[9] Wang M L, Choong Y M, Su N W, et al. J Food Drug Anal, 2003, 11(2):133
[10] Lu L, Gong X, Feng Y L. Chinese Journal of Chromatography, 2014, 32(11):1286芦丽, 宫旭, 冯有龙. 色谱, 2014, 32(11):1286
[11] Russo M V, Goretti G C, Liberti A. HRC CC J High Resolut Chromatogr Chromatogr Commun, 1985, 8(9):535
[12] Cartoni G P, Castellani L, Goretti G, et al. J Chromatogr A, 1991, 552(1/2):197
[13] Rodríguez-Sánchez S, Galindo-Iranzo P, Soria A C, et al. J Chromatogr A, 2014, 1326:96
[14] Bruner F A, Carton G P, Liberti A. Advances in Chromatography. Florida:Chemical Rubber Company Press, 1966
[15] Berezkin V G, Zeeuw J D. Capillary Gas Adsorption Chromatography. Heidelberg:Hüth GmbH, 1996

Preparation and performance evaluation of chromatographic column precoated with graphitized carbon black

PDF

Knowledge

Abstract

Cite this article

share this article

share this article

References

Related Articles 15

Recommended Articles

Metrics

[1]	DU Jie, SUN Pengchao, ZHANG Menglu, LIAN Zete, YUAN Fenggang, WANG Gang. Preparation of porous boron nitride-doped polypyrrole-2,3,3-trimethylindole solid-phase microextraction coating for polycyclic aromatic hydrocarbon detection [J]. Chinese Journal of Chromatography, 2023, 41(9): 789-798.
[2]	QU Jian, NI Yuwen, YU Haoran, TIAN Hongxu, WANG Longxing, CHEN Jiping. New pretreatment method for detecting petroleum hydrocarbons in soil: silica-gel dehydration and cyclohexane extraction [J]. Chinese Journal of Chromatography, 2023, 41(9): 814-820.
[3]	LU Huiyuan, WANG Lijuan, ZHANG Jiongkai, ZHANG Chizhong, LI Tianjuan, JI Ruixue, SHEN Weijian. Determination of four fatty acid ethyl esters in olive oil by solid phase extraction-gas chromatography [J]. Chinese Journal of Chromatography, 2023, 41(4): 359-365.
[4]	ZHANG Zhenyong. Chiral capillary gas chromatography for the separation of the enantiomers of 4-chloromethyl-2,2-dimethyl-1,3-dioxolane [J]. Chinese Journal of Chromatography, 2023, 41(12): 1135-1140.
[5]	YANG Han, TANG Wenqi, ZENG Chu, MENG Shasha, XU Ming. Rational design of high performance metal organic framework stationary phase for gas chromatography [J]. Chinese Journal of Chromatography, 2023, 41(10): 853-865.
[6]	CHEN Jia, QIU Hongdeng. Recent advances in carbon dots-based chromatographic separation materials [J]. Chinese Journal of Chromatography, 2023, 41(10): 825-834.
[7]	HONG Haixiang, ZANG Kunpeng, CHEN Yuanyuan, LIN Yi, LI Jiaxin, QING Xuemei, QIU Shanshan, XIONG Haoyu, JIANG Kai, FANG Shuangxi. Monitoring of atmospheric CH₄, CO, CO₂, N₂O and SF₆ using three-channel gas chromatography [J]. Chinese Journal of Chromatography, 2022, 40(8): 763-771.
[8]	SUN Yinlu, WANG Lin, YIN Zhiyu, ZHAO Jianwei. Simulation of gas chromatographic separation based on random diffusion [J]. Chinese Journal of Chromatography, 2022, 40(3): 281-288.
[9]	ZHANG Han, LIAO Xu, WEI Lai, ZHANG Zixing, REN Hongyun, ZHANG Xian. Design and application of online derivatization device for polar organics on atmospheric particulate filter [J]. Chinese Journal of Chromatography, 2022, 40(1): 100-106.
[10]	SHEN Zhaodong, HUANG Dongmei, FANG Changling, YE Hongli, TIAN Liangliang, WU Zi, ZHANG Jun. Determination of fatty acids compositions and contents in Chinese mitten crabs by gas chromatography [J]. Chinese Journal of Chromatography, 2021, 39(12): 1340-1346.
[11]	TANG Wenqi, MENG Shasha, XU Ming, GU Zhiyuan. Application of gas chromatography separation based on metal-organic framework material as stationary phase [J]. Chinese Journal of Chromatography, 2021, 39(1): 57-68.
[12]	CHEN Dongyang, ZHANG Hao, FENG Jiali, ZENG Dong. Advances in technologies for determination of illegal drugs in health food [J]. Chinese Journal of Chromatography, 2020, 38(8): 880-890.
[13]	HU Yawei, YANG Yang, PENG Jinfeng. Research progress on detection of 2-acetyl-1-pyrroline, the characteristic aroma component of fragrant rice [J]. Chinese Journal of Chromatography, 2020, 38(7): 768-774.
[14]	YANG Ren, WANG Jinxing, ZHANG Yue, WANG Qing, YUE Xuanfeng. Gas chromatographic determination of trace carbon monoxide and carbon dioxide in sulfur hexafluoride and its application to probing potential breakdown of high-voltage circuit breaker [J]. Chinese Journal of Chromatography, 2020, 38(6): 702-707.
[15]	HE Yongrui, QI Meiling. Advances in stationary phases for gas chromatography [J]. Chinese Journal of Chromatography, 2020, 38(4): 409-413.