色谱

	Latest issue 2008 Vol.26 (Number 5) Oct. 27, 2008
	Articles

	技术与应用

Articles

	529	HU Zhixiong, , ZHANG Weinong, HE Haibo, FENG Yuqi and DA Shilu
		Preparation of magnesia-zirconia based mimetic biomembrane stationary phase and its applications in evaluating drug-membrane interactions
		A novel mimetic biomembrane chromatographic stationary phase of magnesia-zirconia composite matrix was prepared based on the Lewis acid-base interaction between the phosphonate group of phosphatidylcholine residue and the Lewis acid sites of magnesia-zir...
		Chinese Journal of Chromatography 26 (5): 529～533 [Abstract ] ( 106 ) [PDF 0KB ]( 0 )

	534	DU Rong, , CHEN Baowen, GUO Lei, LI Yang, XIE Jianwei, WANG Guozhi and ZHOU Hongbing
		Identification of Mycobacterium species using reversed-phase high performance liquid chromatographic analysis of mycolic acid
		A method for the identification of Mycobacterium species using reversed-phase high performance liquid chromatography (RP-HPLC) was developed. The fingerprints library was constructed on the basis of RP-HPLC chromatograms of the mycolic acids derivatives f...
		Chinese Journal of Chromatography 26 (5): 534～539 [Abstract ] ( 85 ) [PDF 0KB ]( 0 )

	540	ZHANG Hongyan, LU Dandan, WU Lixia, ZHOU Zhe and WANG Shengqi
		Analysis of the related substances in phosphorothioate antisense oligonucleotide FT19
		A method using anion exchange high performance liquid chromatography (AX-HPLC) and capillary gel electrophoresis (CGE) was established for the analysis of the related substances in phosphorothioate antisense oligonucleotide FT19 for quality control. The ...
		Chinese Journal of Chromatography 26 (5): 540～543 [Abstract ] ( 72 ) [PDF 0KB ]( 0 )

	544	SULTANA Najma, ARAYNE M Saeed, ALI S Shahid and SAJID Shahnawaz
		Simultaneous determination of olmesartan medoxomil and irbesartan and hydrochlorothiazide in pharmaceutical formulations and human serum using high performance liquid chromatography
		A simple, selective, sensitive, precise, simultaneous high performance liquid chromatographic analysis of serum samples and commercial tablet formulation containing hydrochlorothiazide, olmesartan medoxomil and irbesartan are reported. Good chromatographi...
		Chinese Journal of Chromatography 26 (5): 544～549 [Abstract ] ( 94 ) [PDF 0KB ]( 0 )

	550	ZHU Weihuang, WU Fengchang and HUANG Tinglin
		Determination of kinetic transformation of two geometrical isomers of the ［Fe(PDT)3］2+ by high performance liquid chromatography
		The kinetic transformation of the two isomers of the ［Fe(PDT)3］2+ (PDT: 3-(2-pyridyl)-5,6-diphenyl-1,2,4-triazine) was studied by high performance liquid chromatography. The transformation between two isomers was proved to be treated kinetically as the ...
		Chinese Journal of Chromatography 26 (5): 550～553 [Abstract ] ( 81 ) [PDF 0KB ]( 0 )

	554	ZHU Huijuan, YANG Yanwei, ZHANG Weiqiang and ZHU Ying
		Determination of 22 components in hair dyes by high performance liquid chromatography
		A high performance liquid chromatographic (HPLC) method was developed for the determination of 22 components in hair dyes. The target analytes were separated on an amide bonded C16 silica column (250 mm×4.6 mm, 5 μm), employing acetonitrile-0.025 mol/L ...
		Chinese Journal of Chromatography 26 (5): 554～558 [Abstract ] ( 79 ) [PDF 0KB ]( 0 )

	559	JIA Shaodong, ZHANG Meina and JIN Dongri
		Resolution of thyroxine hormone enantiomers by precolumn derivatization with a fluorescent chiral reagent using reversed-phase high performance liquid chromatography
		A highly fluorescent chiral tagging reagent, R(-)-4-(N,N-dimethylaminosulfonyl)-7-(3-isothiocy-anatopyrrolidino)-2,1,3-benzoxadiazole （R(-)-DBD-PyNCS）, was employed for the enantiomer separation of thyroxine hormone, D,L-3,5,3′,5′-tetraiodothyronine ...
		Chinese Journal of Chromatography 26 (5): 559～562 [Abstract ] ( 85 ) [PDF 0KB ]( 0 )

	563	HE Qiang, KONG Xianghong, ZHAO Jie, LI Jianhua, YUE Aishan and ZHANG Ying
		Determination of benomyl, carbendazim and thiabendazole in apple juice concentrate using solid-phase extraction coupled with ion exchange chromatography
		A method was developed for the determination of benomyl, carbendazim and thiabendazole in apple juice concentrate by solid-phase extraction coupled with ion exchange chromatography (IEC). The sample was diluted with water, and then benomyl was degradated ...
		Chinese Journal of Chromatography 26 (5): 563～567 [Abstract ] ( 79 ) [PDF 0KB ]( 0 )

	568	LOU Zhengyun, CHEN Zongmao, LUO Fengjian, TANG Fubin and LIU Guangming
		Determination of 92 pesticide residues in tea by gas chromatography with solid-phase extraction
		A multiresidue analytical method was developed for the determination of ninety-two pesticides in tea using solid-phase extraction (SPE) and gas chromatographic determination. Tea samples were extracted with acetonitrile, organophosphorus pesticides were c...
		Chinese Journal of Chromatography 26 (5): 568～576 [Abstract ] ( 85 ) [PDF 0KB ]( 0 )

	577	WU Gang, , BAO Xiaoxia, WANG Huaxiong, YU Chunyan, WU Huiming and YE Qingfu
		A rapid multi-residual analysis for organophosphorus pesticides in the products of animal origin using gas chromatography coupled with accelerated solvent extraction and gel permeation chromatographic purification
		A rapid method has been developed to determine the multi-residues of 36 organophosphorus pesticides in the products of animal origin using capillary gas chromatography with flame photometric detector (GC-FPD (P)). The organophosphorus pesticides were extr...
		Chinese Journal of Chromatography 26 (5): 577～582 [Abstract ] ( 88 ) [PDF 0KB ]( 0 )

	583	FAN Yuanmu, HUANG Shaotang, YU Xuejun, GU Xiaojun, QIU Yajun, ZHAN Jia, CHEN Shubing, HE Xiaoyu, CHEN Jun, WANG Shijie, LI Yaping and LI Zhongbang
		Determination of 28 organochlorine and synthetic pyrethroid pesticides in greasy wool using accelerated solvent extraction technique and gas chromatography
		A method for the simultaneous determination of 28 organochlorine and synthetic pyrethroid pesticides in greasy wool was developed by accelerated solvent extraction (ASE) coupled with gas chromatography-electron capture detection (GC-ECD). The organochlori...
		Chinese Journal of Chromatography 26 (5): 583～589 [Abstract ] ( 80 ) [PDF 0KB ]( 0 )

	590	YAO Guiyan, GUAN Wenna, XU Feng, WANG Hua and GUAN Yafeng
		Analysis of phenolic compounds in aqueous samples by gas chromatography coupled with headspace solid-phase microextraction using poly(phthalazine ether sulfone ketone) coated fiber
		The direct trace analysis of phenolic compounds in aqueous samples was performed by headspace solid-phase microextraction/gas chromatography (HS-SPME/GC). A laboratory made poly(phthalazine ether sulfone ketone) (PPESK, 30 μm) coated fiber was used to ex...
		Chinese Journal of Chromatography 26 (5): 590～594 [Abstract ] ( 71 ) [PDF 0KB ]( 0 )

	595	XIA Jingen, CHEN Bo and YAO Shouzhuo
		Determination of hydroxyproline in collagenous proteins by high performance liquid chromatography-mass spectrometry
		A simple, rapid and accurate method for the determination of hydroxyproline in collagenous proteins by high performance liquid chromatography-electrospray mass spectrometry (HPLC-ESI/MS) was developed. After hydrolysis of collagenous proteins with hydroch...
		Chinese Journal of Chromatography 26 (5): 595～598 [Abstract ] ( 60 ) [PDF 0KB ]( 0 )

	599	XU Haitang, HUANG Lihan, XU Yuanjin and
		Simultaneous determination of five effective components in Qingrejiedu oral liquid using high performance liquid chromatography-mass spectrometry
		A high performance liquid chromatography-electrospray ionization mass spectrometry (HPLC-ESI/MS) method for the simultaneous determination of five effective components in Qingrejiedu oral liquid was developed. The HPLC separation was performed on a Zorba...
		Chinese Journal of Chromatography 26 (5): 599～602 [Abstract ] ( 77 ) [PDF 0KB ]( 0 )

	603	DING Youchao, CAO Xizhong, WU Lina and ZHANG Qian
		Fast separation and identification of nine carcinogenic dyes in textiles using liquid chromatography-electrospray tandem mass spectrometry
		A qualitative method of the identification of nine carcinogenic dyes prohibited in textiles was developed using high performance liquid chromatography-tandem mass spectrometry interfaced with electro-spray ionization (HPLC-ESI-MS/MS) in the selective reac...
		Chinese Journal of Chromatography 26 (5): 603～607 [Abstract ] ( 67 ) [PDF 0KB ]( 0 )

	618	HUANG Cheng, JIANG Liying, CHEN Jianmeng and CHEN Xiao
		Determination of environmental estrogens in pharmacy wastewater using solid-phase extraction-gas chromatography/mass spectrometry with derivatization
		A method for the determination of estrone (E1), estradiol (E2), ethinylestradiol (EE2) and estriol (E3) in pharmacy wastewater was developed using solid-phase extraction-gas chromatography/mass spectrometry （SPE-GC/MS） with derivatization. The sample wa...
		Chinese Journal of Chromatography 26 (5): 618～621 [Abstract ] ( 66 ) [PDF 0KB ]( 0 )

	622	WU Jin, FAN Liuyin, ZHANG Wei, WANG Qiuling and CAO Chengxi
		Urine profiling by capillary electrophoresis with online stacking of moving reaction boundary
		Rapid and sensitive profiling of urine holds evident significance for the discovery of new biomarkers and clinical diagnosis. In this study, a simple, rapid and sensitive moving reaction boundary (MRB)-induced stacking technique is described for the analy...
		Chinese Journal of Chromatography 26 (5): 622～625 [Abstract ] ( 74 ) [PDF 0KB ]( 0 )

	626	PAN Yuanyuan, LIANG Lina, CAI Yaqi and MOU Shifen
		Analyse of sugars in beer and wort using high performance anion-exchange chromatography coupled with pulsed amperometric detection
		The method of the simultaneous and direct analysis of eleven sugars, including monosaccharides, disaccharides and oligosaccharides, was established using high performance anion-exchange chromatography (HPAEC) coupled with pulsed amperometric detection (PA...
		Chinese Journal of Chromatography 26 (5): 626～630 [Abstract ] ( 77 ) [PDF 0KB ]( 0 )

	608	HU Beizhen, SONG Weihua, XIE Liping and SHAO Tiefeng
		Determination of 14 pesticide residues in sulfur-containing vegetables by gas chromatography-negative chemical ionization mass spectrometry
		A gas chromatography-negative chemical ionization mass spectrometric (GC-NCI/MS) method has been developed for analyzing 14 pesticide residues in sulfur-containing vegetables (scallion, garlic, garlic bolt, leek, etc.). The samples were first heated in a ...
		Chinese Journal of Chromatography 26 (5): 608～612 [Abstract ] ( 79 ) [PDF 0KB ]( 0 )

	613	WANG Lili, WANG Cong, PAN Zaifa and SUN Fa
		Pyrolysis-gas chromatographic fingerprints with hierarchical cluster analysis for Dendrobium candidum Wall. ex Lindl.
		The pyrogram fingerprints of Dendrobium candidum Wall. ex Lindl. from different regions were studied by pyrolysis-gas chromatography/mass spectrometry (Py-GC/MS) and compared with hierarchical cluster analysis. The effect of pyrolysis temperature on the f...
		Chinese Journal of Chromatography 26 (5): 613～617 [Abstract ] ( 76 ) [PDF 0KB ]( 0 )

技术与应用

	631	HAN Xiaoqian, WEI Yan, LIU Yanhua, CHANG Jing, QIU Wei and CHEN Feng
		Chiral separation of racemic epoxiconazole on cellulose tris(3,5-dimethylphenylcarbamate) chiral stationary phase using high performance liquid chromatography
		The two pairs of enantiomers of epoxiconazole were resolved using normal phase, reversed-phase and polar organic solvent high performance liquid chromatography on cellulose tris(3,5-dimethylphenylcarbamate) (CDMPC) chiral stationary phase, separately. The...
		Chinese Journal of Chromatography 26 (5): 631～633 [Abstract ] ( 71 ) [PDF 0KB ]( 0 )

	634	XIE Huiming, WU Fangrui, YANG Yi and LIU Jie
		Determination of 1-deoxynojirimycin in Morus alba L. leaves using reversed-phase high performance liquid chromatography-fluorescence detection with pre-column derivatization
		A rapid, reliable and suitable method for the determination of 1-deoxynojirimycin (DNJ) in Morus alba L. leaves has been developed. The DNJ in 100 mg dried leaves was extracted twice with 10 mL aqueous 0.05 mol/L HCl, then derivatized by 6-aminoquinoiyi-...
		Chinese Journal of Chromatography 26 (5): 634～636 [Abstract ] ( 76 ) [PDF 0KB ]( 0 )

	637	SHOU Dan, DAI Shiwen, ZHANG Jianmin, LI Hongyu and YU Zhongming
		Simultaneous determination of atractylenolide Ⅲ, atractylenolideⅠ and atractylon in Artactylodis
		A microbore liquid chromatography (microbore LC) has been developed for the simultaneous determination of atractylenolide Ⅲ, atractylenolideⅠ and atractylon in Artactylodis macrocephala. In the method, a Microsil C18 column (150 mm×1.0 mm) was used wi...
		Chinese Journal of Chromatography 26 (5): 637～639 [Abstract ] ( 76 ) [PDF 0KB ]( 0 )

	640	ZHANG Chunhong, , ZHAO Yingchun, HAN Chunhui and GUO Xingjie
		Simultaneous determination of adapalene, 2-phenoxyethanol and methyl-4-hydroxybenzoate in adapalene gels using high performance liquid chromatography
		A reversed-phase high performance liquid chromatographic (RP-HPLC) method was developed for the simultaneous determination of the contents of adapalene and the preservatives (2-phenoxyethanol and methyl-4-hydroxybenzoate) in adapalene gels. The chromatogr...
		Chinese Journal of Chromatography 26 (5): 640～642 [Abstract ] ( 86 ) [PDF 0KB ]( 0 )

	643	CHEN Yuqing, MA Zheng, AN Fang and GUO Xingjie
		Enantiomeric separation of liarozole on amylose chiral stationary phase
		A high performance liquid chromatographic method was established for the enantiomeric separation of liarozole. Baseline chiral separation of liarozole was achieved under normal-phase chromatographic mode by the Chiralpak AD-H chiral stationary phase. The ...
		Chinese Journal of Chromatography 26 (5): 643～645 [Abstract ] ( 82 ) [PDF 222KB ]( 0 )

	646	YANG Yang, CHEN Jianhai, CHANG Liping and HUANG Qi
		Determination of decabromodiphenyl ethane using high performance liquid chromatography
		A method was developed for the quantitative determination of decabromodiphenyl ethane (DBDPE) using high performance liquid chromatography (HPLC). The sample was separated on a Zorbax C18 column (5 μm, 150 mm×4.6 mm) at the temperature of 40 ℃ with t...
		Chinese Journal of Chromatography 26 (5): 646～648 [Abstract ] ( 80 ) [PDF 0KB ]( 0 )

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