]*>","")" /> 高效液相色谱法测定间乙酰氨基苯胺中杂质含量

色谱

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高效液相色谱法测定间乙酰氨基苯胺中杂质含量

洪成清,   

  • 出版日期:1994-07-30 发布日期:1999-04-25

  • Online:1994-07-30 Published:1999-04-25

摘要: An HPLC method for determination of l,3-diaminobenzene and N,N'-diacetyl-l,3-diaminobenzene in m-aminoacetanilide was developed.The column used was μ-Bondapak C_(18) with UV detector at 239 nm. The mo-bile phase was methanol-phosphate buffer solution(35 : 65, pH 6.5).The determination was based on the ex-ternal standard method.In the concentration range of l~15μg/mL calibration curves were linear.

关键词: N.N'-二乙酰替间苯二胺, 高效液相色谱, 间苯二胺, 间乙酰氨基苯胺.

Key words: NULL