]*>","")" /> 高效液相色谱法测定22S，23S，24R表高油菜素内酯
色谱

色谱

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高效液相色谱法测定22S，23S，24R表高油菜素内酯

刘国清,张洪彬,刘建平,李良   

  • 出版日期:1995-07-30 发布日期:1998-04-25

  • Online:1995-07-30 Published:1998-04-25

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摘要： The sample was dissolved in ethyl acetate and reactcd with pbenylboronic acid at 80°for 3Omin.Then itwas detemined by HPLC using UV detector at 222nm. The linear relations between the amounts and thepeak areas in the range of 0. 02mg/mL to 0.12mg/mL were staisfactory(γ=0. 9999,n=6). Average recovery was 99.27%～101.5%.

关键词: 高效液相色谱法, 油菜素内酯, 柱前衍生化

Key words: NULL