Chinese Journal of Chromatography ›› 2023, Vol. 41 ›› Issue (6): 457-471.DOI: 10.3724/SP.J.1123.2022.09027
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WANG Xuemei(), HUANG Lixia, YUAN Na, HUANG Pengfei, DU Xinzhen, LU Xiaoquan
Received:
2022-09-29
Online:
2023-06-08
Published:
2023-06-01
Supported by:
CLC Number:
WANG Xuemei, HUANG Lixia, YUAN Na, HUANG Pengfei, DU Xinzhen, LU Xiaoquan. Progress in preparation of hollow nanomaterials and their application to sample pretreatment[J]. Chinese Journal of Chromatography, 2023, 41(6): 457-471.
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URL: https://www.chrom-china.com/EN/10.3724/SP.J.1123.2022.09027
Fig. 7 (a) Schematic illustration of the formation of ZnO hollow microspheres and (b-e) the evolution of ZnO hollow microspheres with solvothermal time of 2, 6, 12, 24 h, respectively[33]
Fig. 9 (a) Schematic illustration of the route for preparing, and (b) unique microstructure and potential applications of montmorillonite hollow and graded mesoporous microspheres (MMTNS@CS-HMPHS)[40]
Fig. 13 Schematic of magnetic solid-phase extraction (MSPE) and preparation process of porous cage-like hollow magnetic carbon doped cobalt oxide nanocomposites (CoO@C)[70]
Method | Type of materials | Analytes | Combined method | Linear range | LODs | Ref. |
---|---|---|---|---|---|---|
SPE | CHPMs | V(Ⅴ), Cr(Ⅲ), Cu(Ⅱ), Cd(Ⅱ), Pb(Ⅱ) | ICP-MS | 0.05-15 μg/L | 0.8-3.2 ng/L | [ |
NiCo2O4 | Pb(Ⅱ) | FAAS | 0.5-10 mg/L | 5.9 μg/L | [ | |
h-PDA@L-lys | BR | HPLC | - | - | [ | |
SPME | HCNCs | PAHs | GC-MS | 5-2000 ng/L | 0.03-0.70 ng/L | [ |
Co3O4/C | PAHs | HPLC | 0.005-1000 μg/L | 0.002-2.680 μg/L | [ | |
Fe2O3/CeO2@MnO2 | PAHs | GC-MS | 0.04-100 μg/L | 0.38-3.57 ng/L | [ | |
MSPE | CoO@C | PAHs | HPLC | 0.5-1000 μg/L | 0.06-1.30 μg/L | [ |
Fe3O4@C | PBDEs | GC-MS | 1-1000 ng/L | 0.07-0.17 ng/L | [ | |
Fe3O4@COFs | DPA | HPLC | 0.1-100 mg/L | 0.02-0.08 mg/L | [ | |
Fe3O4@MIL-100 | triclosan | HPLC | 0.1-50 mg/kg | 0.03 mg/kg | [ | |
DSPE | BNHSs | PCBs | GC-MS | 0.15-250 ng/L | 0.04-0.09 ng/L | [ |
In2S3@MIL-125(Ti) | NPAHs | GC-MS | 10-1000 ng/L | 2.9-83.0 ng/L | [ |
Table 1 Application of hollow nanomaterials in sample pretreatment
Method | Type of materials | Analytes | Combined method | Linear range | LODs | Ref. |
---|---|---|---|---|---|---|
SPE | CHPMs | V(Ⅴ), Cr(Ⅲ), Cu(Ⅱ), Cd(Ⅱ), Pb(Ⅱ) | ICP-MS | 0.05-15 μg/L | 0.8-3.2 ng/L | [ |
NiCo2O4 | Pb(Ⅱ) | FAAS | 0.5-10 mg/L | 5.9 μg/L | [ | |
h-PDA@L-lys | BR | HPLC | - | - | [ | |
SPME | HCNCs | PAHs | GC-MS | 5-2000 ng/L | 0.03-0.70 ng/L | [ |
Co3O4/C | PAHs | HPLC | 0.005-1000 μg/L | 0.002-2.680 μg/L | [ | |
Fe2O3/CeO2@MnO2 | PAHs | GC-MS | 0.04-100 μg/L | 0.38-3.57 ng/L | [ | |
MSPE | CoO@C | PAHs | HPLC | 0.5-1000 μg/L | 0.06-1.30 μg/L | [ |
Fe3O4@C | PBDEs | GC-MS | 1-1000 ng/L | 0.07-0.17 ng/L | [ | |
Fe3O4@COFs | DPA | HPLC | 0.1-100 mg/L | 0.02-0.08 mg/L | [ | |
Fe3O4@MIL-100 | triclosan | HPLC | 0.1-50 mg/kg | 0.03 mg/kg | [ | |
DSPE | BNHSs | PCBs | GC-MS | 0.15-250 ng/L | 0.04-0.09 ng/L | [ |
In2S3@MIL-125(Ti) | NPAHs | GC-MS | 10-1000 ng/L | 2.9-83.0 ng/L | [ |
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